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Tie Dye Instructions. 1) Choose an item made of cotton and white. 100% cotton works best. It is okay if it has words on it. (Shirt, socks,. Be sure to follow the instructions on the dye's package for best dyeing and color results. IMPORTANT NOTE ABOUT DYES: Dye maintains its potency for only 48-72LET IT SET. Let set for 6-8 hours or longer for most intense colors. RINSE IT OUT. Rinse well with water until excess dye is removed. Cut rubber bands if used.